| Bruker X8 APEX diffractometer | 5347 independent reflections |
| Radiation source: fine-focus sealed tube | 4118 reflections with I > 2σ(I) |
| Graphite monochromator | Rint = 0.031 |
| φ and ω scans | θmax = 29.6°, θmin = 2.2° |
| Absorption correction: multi-scan (SADABS; Sheldrick, 1995) | h = −16→16 |
| Tmin = 0.673, Tmax = 0.746 | k = −25→25 |
| 38870 measured reflections | l = −8→12 |