| Crystal data |
| Chemical formula |
C36H42O8
|
|
M
r
|
602.69 |
| Crystal system, space group |
Triclinic, P
|
| Temperature (K) |
90 |
|
a, b, c () |
10.9358(6), 11.6121(6), 13.6833(7) |
| , , () |
72.148(2), 86.447(2), 66.766(2) |
|
V (3) |
1516.36(14) |
|
Z
|
2 |
| Radiation type |
Mo K
|
| (mm1) |
0.09 |
| Crystal size (mm) |
0.32 0.27 0.16 |
| |
| Data collection |
| Diffractometer |
Bruker D8 Venture |
| Absorption correction |
Multi-scan (SADABS; Bruker, 2014 ▸) |
|
T
min, T
max
|
0.97, 0.98 |
| No. of measured, independent and observed [I > 2(I)] reflections |
27885, 5346, 4078 |
|
R
int
|
0.052 |
| (sin /)max (1) |
0.595 |
| |
| Refinement |
|
R[F
2 > 2(F
2)], wR(F
2), S
|
0.047, 0.120, 1.04 |
| No. of reflections |
5346 |
| No. of parameters |
402 |
| H-atom treatment |
H-atom parameters constrained |
|
max, min (e 3) |
0.59, 0.23 |
