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. 2015 Apr 22;71(Pt 5):o324–o325. doi: 10.1107/S2056989015007434
Br1—C5 1.9014 (15) C7—H7 0.9500
O1—C2 1.3418 (19) C8—C16 1.493 (2)
O1—H1 0.8400 C8—C9 1.4956 (19)
O2—C9 1.2221 (19) C9—C10 1.481 (2)
O3—C16 1.218 (2) C10—C11 1.387 (2)
C1—C6 1.412 (2) C10—C15 1.390 (2)
C1—C2 1.417 (2) C11—C12 1.390 (2)
C1—C7 1.449 (2) C11—H11 0.9500
C2—C3 1.398 (2) C12—C13 1.399 (3)
C3—C4 1.377 (2) C12—H12 0.9500
C3—H3 0.9500 C13—C14 1.390 (2)
C4—C5 1.393 (2) C13—H13 0.9500
C4—H4 0.9500 C14—C15 1.390 (2)
C5—C6 1.378 (2) C14—H14 0.9500
C6—H6 0.9500 C15—C16 1.490 (2)
C7—C8 1.355 (2)
C2—O1—H1 113.9 O2—C9—C10 124.70 (14)
C6—C1—C2 118.43 (14) O2—C9—C8 127.73 (14)
C6—C1—C7 125.05 (14) C10—C9—C8 107.57 (13)
C2—C1—C7 116.51 (14) C11—C10—C15 121.66 (15)
O1—C2—C3 121.74 (14) C11—C10—C9 129.07 (15)
O1—C2—C1 117.73 (13) C15—C10—C9 109.27 (13)
C3—C2—C1 120.53 (14) C10—C11—C12 117.32 (15)
C4—C3—C2 120.16 (14) C10—C11—H11 121.3
C4—C3—H3 119.9 C12—C11—H11 121.3
C2—C3—H3 119.9 C11—C12—C13 121.16 (15)
C3—C4—C5 119.47 (14) C11—C12—H12 119.4
C3—C4—H4 120.3 C13—C12—H12 119.4
C5—C4—H4 120.3 C14—C13—C12 121.23 (15)
C6—C5—C4 121.94 (14) C14—C13—H13 119.4
C6—C5—Br1 119.65 (12) C12—C13—H13 119.4
C4—C5—Br1 118.37 (11) C13—C14—C15 117.44 (15)
C5—C6—C1 119.46 (14) C13—C14—H14 121.3
C5—C6—H6 120.3 C15—C14—H14 121.3
C1—C6—H6 120.3 C14—C15—C10 121.19 (15)
C8—C7—C1 134.39 (15) C14—C15—C16 128.67 (15)
C8—C7—H7 112.8 C10—C15—C16 110.15 (14)
C1—C7—H7 112.8 O3—C16—C15 124.43 (15)
C7—C8—C16 133.85 (14) O3—C16—C8 128.87 (14)
C7—C8—C9 119.83 (14) C15—C16—C8 106.70 (13)
C16—C8—C9 106.32 (13)
C6—C1—C2—O1 178.65 (15) C8—C9—C10—C11 −179.35 (16)
C7—C1—C2—O1 −2.4 (2) O2—C9—C10—C15 179.00 (16)
C6—C1—C2—C3 −0.7 (2) C8—C9—C10—C15 −0.22 (18)
C7—C1—C2—C3 178.19 (15) C15—C10—C11—C12 0.3 (2)
O1—C2—C3—C4 −178.38 (17) C9—C10—C11—C12 179.34 (16)
C1—C2—C3—C4 1.0 (3) C10—C11—C12—C13 −0.3 (3)
C2—C3—C4—C5 −0.7 (3) C11—C12—C13—C14 0.0 (3)
C3—C4—C5—C6 0.1 (3) C12—C13—C14—C15 0.4 (3)
C3—C4—C5—Br1 −177.54 (13) C13—C14—C15—C10 −0.4 (3)
C4—C5—C6—C1 0.1 (2) C13—C14—C15—C16 −179.70 (17)
Br1—C5—C6—C1 177.74 (12) C11—C10—C15—C14 0.1 (3)
C2—C1—C6—C5 0.2 (2) C9—C10—C15—C14 −179.15 (15)
C7—C1—C6—C5 −178.61 (15) C11—C10—C15—C16 179.48 (15)
C6—C1—C7—C8 −1.5 (3) C9—C10—C15—C16 0.27 (19)
C2—C1—C7—C8 179.65 (18) C14—C15—C16—O3 −1.4 (3)
C1—C7—C8—C16 −0.2 (3) C10—C15—C16—O3 179.24 (17)
C1—C7—C8—C9 −179.21 (17) C14—C15—C16—C8 179.14 (17)
C7—C8—C9—O2 0.1 (3) C10—C15—C16—C8 −0.22 (19)
C16—C8—C9—O2 −179.12 (17) C7—C8—C16—O3 1.5 (3)
C7—C8—C9—C10 179.33 (15) C9—C8—C16—O3 −179.35 (18)
C16—C8—C9—C10 0.08 (17) C7—C8—C16—C15 −179.02 (18)
O2—C9—C10—C11 −0.1 (3) C9—C8—C16—C15 0.08 (17)