| Br1—C5 | 1.9014 (15) | C7—H7 | 0.9500 |
| O1—C2 | 1.3418 (19) | C8—C16 | 1.493 (2) |
| O1—H1 | 0.8400 | C8—C9 | 1.4956 (19) |
| O2—C9 | 1.2221 (19) | C9—C10 | 1.481 (2) |
| O3—C16 | 1.218 (2) | C10—C11 | 1.387 (2) |
| C1—C6 | 1.412 (2) | C10—C15 | 1.390 (2) |
| C1—C2 | 1.417 (2) | C11—C12 | 1.390 (2) |
| C1—C7 | 1.449 (2) | C11—H11 | 0.9500 |
| C2—C3 | 1.398 (2) | C12—C13 | 1.399 (3) |
| C3—C4 | 1.377 (2) | C12—H12 | 0.9500 |
| C3—H3 | 0.9500 | C13—C14 | 1.390 (2) |
| C4—C5 | 1.393 (2) | C13—H13 | 0.9500 |
| C4—H4 | 0.9500 | C14—C15 | 1.390 (2) |
| C5—C6 | 1.378 (2) | C14—H14 | 0.9500 |
| C6—H6 | 0.9500 | C15—C16 | 1.490 (2) |
| C7—C8 | 1.355 (2) | ||
| C2—O1—H1 | 113.9 | O2—C9—C10 | 124.70 (14) |
| C6—C1—C2 | 118.43 (14) | O2—C9—C8 | 127.73 (14) |
| C6—C1—C7 | 125.05 (14) | C10—C9—C8 | 107.57 (13) |
| C2—C1—C7 | 116.51 (14) | C11—C10—C15 | 121.66 (15) |
| O1—C2—C3 | 121.74 (14) | C11—C10—C9 | 129.07 (15) |
| O1—C2—C1 | 117.73 (13) | C15—C10—C9 | 109.27 (13) |
| C3—C2—C1 | 120.53 (14) | C10—C11—C12 | 117.32 (15) |
| C4—C3—C2 | 120.16 (14) | C10—C11—H11 | 121.3 |
| C4—C3—H3 | 119.9 | C12—C11—H11 | 121.3 |
| C2—C3—H3 | 119.9 | C11—C12—C13 | 121.16 (15) |
| C3—C4—C5 | 119.47 (14) | C11—C12—H12 | 119.4 |
| C3—C4—H4 | 120.3 | C13—C12—H12 | 119.4 |
| C5—C4—H4 | 120.3 | C14—C13—C12 | 121.23 (15) |
| C6—C5—C4 | 121.94 (14) | C14—C13—H13 | 119.4 |
| C6—C5—Br1 | 119.65 (12) | C12—C13—H13 | 119.4 |
| C4—C5—Br1 | 118.37 (11) | C13—C14—C15 | 117.44 (15) |
| C5—C6—C1 | 119.46 (14) | C13—C14—H14 | 121.3 |
| C5—C6—H6 | 120.3 | C15—C14—H14 | 121.3 |
| C1—C6—H6 | 120.3 | C14—C15—C10 | 121.19 (15) |
| C8—C7—C1 | 134.39 (15) | C14—C15—C16 | 128.67 (15) |
| C8—C7—H7 | 112.8 | C10—C15—C16 | 110.15 (14) |
| C1—C7—H7 | 112.8 | O3—C16—C15 | 124.43 (15) |
| C7—C8—C16 | 133.85 (14) | O3—C16—C8 | 128.87 (14) |
| C7—C8—C9 | 119.83 (14) | C15—C16—C8 | 106.70 (13) |
| C16—C8—C9 | 106.32 (13) | ||
| C6—C1—C2—O1 | 178.65 (15) | C8—C9—C10—C11 | −179.35 (16) |
| C7—C1—C2—O1 | −2.4 (2) | O2—C9—C10—C15 | 179.00 (16) |
| C6—C1—C2—C3 | −0.7 (2) | C8—C9—C10—C15 | −0.22 (18) |
| C7—C1—C2—C3 | 178.19 (15) | C15—C10—C11—C12 | 0.3 (2) |
| O1—C2—C3—C4 | −178.38 (17) | C9—C10—C11—C12 | 179.34 (16) |
| C1—C2—C3—C4 | 1.0 (3) | C10—C11—C12—C13 | −0.3 (3) |
| C2—C3—C4—C5 | −0.7 (3) | C11—C12—C13—C14 | 0.0 (3) |
| C3—C4—C5—C6 | 0.1 (3) | C12—C13—C14—C15 | 0.4 (3) |
| C3—C4—C5—Br1 | −177.54 (13) | C13—C14—C15—C10 | −0.4 (3) |
| C4—C5—C6—C1 | 0.1 (2) | C13—C14—C15—C16 | −179.70 (17) |
| Br1—C5—C6—C1 | 177.74 (12) | C11—C10—C15—C14 | 0.1 (3) |
| C2—C1—C6—C5 | 0.2 (2) | C9—C10—C15—C14 | −179.15 (15) |
| C7—C1—C6—C5 | −178.61 (15) | C11—C10—C15—C16 | 179.48 (15) |
| C6—C1—C7—C8 | −1.5 (3) | C9—C10—C15—C16 | 0.27 (19) |
| C2—C1—C7—C8 | 179.65 (18) | C14—C15—C16—O3 | −1.4 (3) |
| C1—C7—C8—C16 | −0.2 (3) | C10—C15—C16—O3 | 179.24 (17) |
| C1—C7—C8—C9 | −179.21 (17) | C14—C15—C16—C8 | 179.14 (17) |
| C7—C8—C9—O2 | 0.1 (3) | C10—C15—C16—C8 | −0.22 (19) |
| C16—C8—C9—O2 | −179.12 (17) | C7—C8—C16—O3 | 1.5 (3) |
| C7—C8—C9—C10 | 179.33 (15) | C9—C8—C16—O3 | −179.35 (18) |
| C16—C8—C9—C10 | 0.08 (17) | C7—C8—C16—C15 | −179.02 (18) |
| O2—C9—C10—C11 | −0.1 (3) | C9—C8—C16—C15 | 0.08 (17) |