| Bruker D8 VENTURE PHOTON 100 CMOS diffractometer | 2510 independent reflections |
| Radiation source: INCOATEC IµS micro–focus source | 2386 reflections with I > 2σ(I) |
| Mirror monochromator | Rint = 0.020 |
| Detector resolution: 10.4167 pixels mm-1 | θmax = 74.5°, θmin = 3.3° |
| ω scans | h = −16→17 |
| Absorption correction: numerical (SADABS; Bruker, 2014) | k = −4→4 |
| Tmin = 0.67, Tmax = 0.84 | l = −29→29 |
| 8943 measured reflections |