| Crystal data |
| Chemical formula |
(C4H7N2)[Sn(C2O4)Cl3(H2O)] |
|
M
r
|
414.19 |
| Crystal system, space group |
Triclinic, P
|
| Temperature (K) |
120 |
|
a, b, c () |
7.4757(9), 8.0857(10), 11.2846(14) |
| , , () |
80.856(8), 83.946(9), 86.587(8) |
|
V (3) |
669.05(14) |
|
Z
|
2 |
| Radiation type |
Ga K, = 1.34139 |
| (mm1) |
13.92 |
| Crystal size (mm) |
0.05 0.04 0.04 |
| |
| Data collection |
| Diffractometer |
Bruker Venture Metaljet |
| Absorption correction |
Multi-scan (SADABS; Krause et al., 2015 ▸) |
|
T
min, T
max
|
0.133, 0.255 |
| No. of measured, independent and observed [I > 2(I)] reflections |
5497, 2520, 1604 |
|
R
int
|
0.112 |
| (sin /)max (1) |
0.619 |
| |
| Refinement |
|
R[F
2 > 2(F
2)], wR(F
2), S
|
0.062, 0.150, 1.07 |
| No. of reflections |
2520 |
| No. of parameters |
156 |
| H-atom treatment |
H-atom parameters constrained |
|
max, min (e 3) |
2.10, 1.23 |
