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. 2015 Apr 22;71(Pt 5):523–527. doi: 10.1107/S2056989015006994
Cl1—C6 1.7360 (16) C9—C14 1.395 (2)
P1—O2 1.4882 (11) C10—H10 0.9500
P1—C2 1.8251 (15) C10—C11 1.389 (2)
P1—C9 1.7982 (15) C11—H11 0.9500
P1—C15 1.8083 (15) C11—C12 1.380 (3)
O1—C1 1.2168 (19) C12—H12 0.9500
C1—C2 1.515 (2) C12—C13 1.377 (3)
C1—C3 1.493 (2) C13—H13 0.9500
C2—H2A 0.9900 C13—C14 1.388 (2)
C2—H2B 0.9900 C14—H14 0.9500
C3—C4 1.399 (2) C15—C16 1.387 (2)
C3—C8 1.394 (2) C15—C20 1.399 (2)
C4—H4 0.9500 C16—H16 0.9500
C4—C5 1.380 (2) C16—C17 1.391 (2)
C5—H5 0.9500 C17—H17 0.9500
C5—C6 1.387 (2) C17—C18 1.383 (3)
C6—C7 1.384 (2) C18—H18 0.9500
C7—H7 0.9500 C18—C19 1.382 (3)
C7—C8 1.388 (2) C19—H19 0.9500
C8—H8 0.9500 C19—C20 1.384 (2)
C9—C10 1.396 (2) C20—H20 0.9500
O2—P1—C2 114.35 (7) C14—C9—C10 119.68 (14)
O2—P1—C9 112.64 (7) C9—C10—H10 120.2
O2—P1—C15 112.02 (7) C11—C10—C9 119.67 (16)
C9—P1—C2 105.04 (7) C11—C10—H10 120.2
C9—P1—C15 106.60 (7) C10—C11—H11 119.9
C15—P1—C2 105.54 (7) C12—C11—C10 120.30 (16)
O1—C1—C2 119.05 (14) C12—C11—H11 119.9
O1—C1—C3 120.86 (14) C11—C12—H12 119.9
C3—C1—C2 120.09 (13) C13—C12—C11 120.22 (16)
P1—C2—H2A 108.9 C13—C12—H12 119.9
P1—C2—H2B 108.9 C12—C13—H13 119.8
C1—C2—P1 113.43 (10) C12—C13—C14 120.44 (16)
C1—C2—H2A 108.9 C14—C13—H13 119.8
C1—C2—H2B 108.9 C9—C14—H14 120.2
H2A—C2—H2B 107.7 C13—C14—C9 119.69 (15)
C4—C3—C1 117.63 (14) C13—C14—H14 120.2
C8—C3—C1 123.27 (14) C16—C15—P1 118.74 (12)
C8—C3—C4 119.09 (15) C16—C15—C20 119.81 (15)
C3—C4—H4 119.4 C20—C15—P1 121.42 (12)
C5—C4—C3 121.18 (15) C15—C16—H16 119.9
C5—C4—H4 119.4 C15—C16—C17 120.17 (15)
C4—C5—H5 120.8 C17—C16—H16 119.9
C4—C5—C6 118.47 (15) C16—C17—H17 120.0
C6—C5—H5 120.8 C18—C17—C16 119.95 (15)
C5—C6—Cl1 119.11 (13) C18—C17—H17 120.0
C7—C6—Cl1 119.12 (13) C17—C18—H18 120.1
C7—C6—C5 121.75 (15) C19—C18—C17 119.88 (16)
C6—C7—H7 120.4 C19—C18—H18 120.1
C6—C7—C8 119.20 (15) C18—C19—H19 119.6
C8—C7—H7 120.4 C18—C19—C20 120.89 (16)
C3—C8—H8 119.9 C20—C19—H19 119.6
C7—C8—C3 120.25 (15) C15—C20—H20 120.4
C7—C8—H8 119.9 C19—C20—C15 119.27 (15)
C10—C9—P1 117.37 (12) C19—C20—H20 120.4
C14—C9—P1 122.92 (12)
Cl1—C6—C7—C8 −176.61 (13) C4—C5—C6—Cl1 177.30 (13)
P1—C9—C10—C11 −177.86 (13) C4—C5—C6—C7 −1.5 (3)
P1—C9—C14—C13 178.80 (13) C5—C6—C7—C8 2.2 (3)
P1—C15—C16—C17 176.49 (12) C6—C7—C8—C3 −0.7 (3)
P1—C15—C20—C19 −176.96 (12) C8—C3—C4—C5 2.2 (2)
O1—C1—C2—P1 97.28 (15) C9—P1—C2—C1 −170.57 (11)
O1—C1—C3—C4 −2.5 (2) C9—P1—C15—C16 −117.67 (13)
O1—C1—C3—C8 178.73 (16) C9—P1—C15—C20 60.42 (14)
O2—P1—C2—C1 65.44 (12) C9—C10—C11—C12 −1.1 (3)
O2—P1—C9—C10 −25.46 (15) C10—C9—C14—C13 1.0 (2)
O2—P1—C9—C14 156.68 (13) C10—C11—C12—C13 1.0 (3)
O2—P1—C15—C16 5.96 (14) C11—C12—C13—C14 0.1 (3)
O2—P1—C15—C20 −175.96 (12) C12—C13—C14—C9 −1.1 (3)
C1—C3—C4—C5 −176.70 (15) C14—C9—C10—C11 0.1 (2)
C1—C3—C8—C7 177.34 (15) C15—P1—C2—C1 −58.14 (12)
C2—P1—C9—C10 −150.53 (13) C15—P1—C9—C10 97.79 (13)
C2—P1—C9—C14 31.61 (15) C15—P1—C9—C14 −80.08 (14)
C2—P1—C15—C16 130.99 (12) C15—C16—C17—C18 0.5 (2)
C2—P1—C15—C20 −50.92 (14) C16—C15—C20—C19 1.1 (2)
C2—C1—C3—C4 176.67 (14) C16—C17—C18—C19 1.2 (3)
C2—C1—C3—C8 −2.1 (2) C17—C18—C19—C20 −1.7 (3)
C3—C1—C2—P1 −81.86 (15) C18—C19—C20—C15 0.6 (3)
C3—C4—C5—C6 −0.7 (2) C20—C15—C16—C17 −1.6 (2)
C4—C3—C8—C7 −1.4 (2)