Table 4. Refinement of the three structures using reduced datasets.

R values from a refinement using conventional monochromatic data are included at the bottom of the table for comparison.

	Sanidine	Cs2[Pt(CN)4]H2O	ZSM-5
No. of reflections	1900	3093	9492
No. of unique reflections	675	1047	2615
Resolution range ()	0.7452.234	0.9162.344	0.9072.653
R int †	0.053	0.097	0.075
R sigma ‡	0.031	0.049	0.040
Completeness (%)§	80	84	80
No. of parameters	64	65	216
R1¶ [F obs > 4(F obs)]	0.069	0.037	0.068
R1¶ (all)	0.074	0.037	0.157
With monochromatic data:
R int †	0.029	0.053	0.049
R1¶ [F obs > 4(F obs)]	0.024	0.020	0.053
R1¶ (all)	0.026	0.020	0.057

^† R _int = | (mean)|/.

^‡ R _sigma = [()]/.

^§Calculated for the resolution range 15.

^¶ R1 = ||| |||/||.