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1H 35 GHz CW ENDOR spectra of Fe3+-HO2R recorded at the two unique g values. Spectra were recorded in H2O (black), D2O (red), or in H2O with 2H-Cys-labeled protein (green). The braces show the range of the proton coupling. Experimental conditions: Temperature, 2 K; Microwave frequency, 34.9 GHz; Modulation amplitude, 2G; RF sweep rate, 1 MHz/s; rf excitation was broadened to 100 kHz.
