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. Author manuscript; available in PMC: 2016 May 13.
Published in final edited form as: J Am Chem Soc. 2015 Apr 30;137(18):5871–5874. doi: 10.1021/jacs.5b02065

Table 3.

γ, δ, ε–C–H Functionalizations of Aliphatic Amidesa,b

graphic file with name nihms688312t3.jpg
a

Conditions: 6 (0.1 mmol), NIS (4 equiv.), TMSN3 (4 equiv.), DCE (1 mL), 100 °C, air, 14 h.

b

Isolated yields.

c

Obtained as a mixture of inseparable mixture of diastereomers (methylene:methyl = 3:1).