Table 1. Data collection and refinement statistics.
DNMT1–USP7 | |
---|---|
Data collection | |
Space group | P212121 |
Cell dimensions | |
a, b, c (Å) | 110.23, 111.62, 163.87 |
α, β, γ (°) | 90, 90, 90 |
Resolution (Å) | 50.0–2.9 (3.0–2.9)* |
Rsym or Rmerge | 14.6 (85.8) |
I/σI | 14.02 (3.86) |
Completeness (%) | 99.19 (92.23) |
Redundancy | 13.8 (13.5) |
Refinement | |
Resolution (Å) | 50.0–2.9 (3.0–2.9) |
No. of reflections | 44396 |
Rwork/Rfree | 20.62/25.64 |
No. of atoms | 11386 |
Protein | 11373 |
Ligand/ion | 2 |
Water | 11 |
B-factors | |
Protein | 66.30 |
Ligand/ion | 67.80 |
Water | 42.50 |
R.m.s. deviations | |
Bond lengths (Å) | 0.003 |
Bond angles (°) | 0.89 |
R.m.s., root-mean-square.
Data set are collected with one native crystal.
*Values in parentheses are for highest-resolution shell.