| Crystal data |
| Chemical formula |
C24H32N4O8S |
|
M
r
|
536.59 |
| Crystal system, space group |
Triclinic, P
|
| Temperature (K) |
100 |
|
a, b, c () |
7.3483(2), 12.2233(3), 13.9847(4) |
| , , () |
95.323(1), 90.281(2), 99.802(1) |
|
V (3) |
1232.16(6) |
|
Z
|
2 |
| Radiation type |
Cu K
|
| (mm1) |
1.67 |
| Crystal size (mm) |
0.15 0.15 0.02 |
| |
| Data collection |
| Diffractometer |
Bruker APEXII CCD area detector |
| Absorption correction |
Multi-scan (SADABS; Bruker, 2008 ▸) |
|
T
min, T
max
|
0.89, 0.97 |
| No. of measured, independent and observed [I > 2(I)] reflections |
15014, 4539, 4292 |
|
R
int
|
0.017 |
| (sin /)max (1) |
0.617 |
| |
| Refinement |
|
R[F
2 > 2(F
2)], wR(F
2), S
|
0.039, 0.111, 1.03 |
| No. of reflections |
4539 |
| No. of parameters |
351 |
| H-atom treatment |
H atoms treated by a mixture of independent and constrained refinement |
|
max, min (e 3) |
0.56, 0.33 |
