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. 2015 Mar 31;137(14):4666–4669. doi: 10.1021/jacs.5b02316

Table 1. Reaction Optimization.

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a

Yields were determined by 1H NMR analysis of the crude reaction mixture using 1,1,2,2-tetrachloroethane as an internal standard.

b

Enantioselectivites were determined by chiral HPLC analysis. ND = not determined. DEMS = (EtO)2MeSiH.