Table 1.
Statistics | MCAK motor domain-peptide complex |
---|---|
Unit cell dimensions | a = 46.31 Å, b = 245.64 Å, c = 79.40 Å, α = 90.00°, β = 95.84°, γ = 90.00° |
Space group | P21 |
Molecules per asymmetric unit | 4 |
Resolution range (Å) | 30.0–3.0 |
Total reflections | 155983 |
Unique reflections | 35,146 |
Completeness (%) | 99.0 (99.2) |
Multiplicity | 4.4 (4.5) |
Rsym (%) | 9.1 (68.2) |
I/σ(I) | 10.2 (2.0) |
Rwork/Rfree (%) | 26.4/28.6 |
Wilson B (Å2) | 77.5 |
Average B (Å2): | |
Overall | 71.0 |
Main chain | 72.05 |
Side chain and solvent | 70.66 |
Peptide | 56.98 |
r.m.s.d. bond lengths (Å) | 0.095 |
r.m.s.d. bond angles (°) | 1.53 |
Ramachandran plot statistics (%): | |
Favoured | 87.6 |
Allowed | 11.7 |
Outliers | 0.7 |