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. 2014 Dec 16;16(3):664–674. doi: 10.1208/s12249-014-0249-x

Table IX.

A Summary of the Reflux and Soxhlet Extractables Data for Unprocessed PVC (μg/g)

Participating Laboratory Type of Extractable Amount measured in the extraction solvent (μg/g)
Hexanea IPA IPA/water Water, pH 2.5 Water Water, pH 9.5
1 DEHP 56,000 67,000 10,000 2 38 40
Sum of extractables 57,007 71,871 10,897 2 55 62
5b DEHP 331,971 261,744 N/A 1 1 N/A
Sum of Extractables 345,176 277,462 N/A 1 4 N/A
3 DEHP 98,325 130,537 164790c 1 1 3
Sum of Extractables 103,646 138,556 175,995 3 4 6

aLab 5 used hexane (described as a mixture of isomers); lab 1 and lab 3 used iso-hexane (2-methylpentane)

bExtraction conditions: Soxhlet extraction, various times for different solvents: 23 h iso-hexane, 23 h IPA, 7 h IPA/H2O, 23 h H2O pH 2.5, 23 h H2O pH 7, 23 h H2O pH 9.5

cSoxhlet extraction

N/A not tested