Table IX.
A Summary of the Reflux and Soxhlet Extractables Data for Unprocessed PVC (μg/g)
Participating Laboratory | Type of Extractable | Amount measured in the extraction solvent (μg/g) | |||||
---|---|---|---|---|---|---|---|
Hexanea | IPA | IPA/water | Water, pH 2.5 | Water | Water, pH 9.5 | ||
1 | DEHP | 56,000 | 67,000 | 10,000 | 2 | 38 | 40 |
Sum of extractables | 57,007 | 71,871 | 10,897 | 2 | 55 | 62 | |
5b | DEHP | 331,971 | 261,744 | N/A | 1 | 1 | N/A |
Sum of Extractables | 345,176 | 277,462 | N/A | 1 | 4 | N/A | |
3 | DEHP | 98,325 | 130,537 | 164790c | 1 | 1 | 3 |
Sum of Extractables | 103,646 | 138,556 | 175,995 | 3 | 4 | 6 |
aLab 5 used hexane (described as a mixture of isomers); lab 1 and lab 3 used iso-hexane (2-methylpentane)
bExtraction conditions: Soxhlet extraction, various times for different solvents: 23 h iso-hexane, 23 h IPA, 7 h IPA/H2O, 23 h H2O pH 2.5, 23 h H2O pH 7, 23 h H2O pH 9.5
cSoxhlet extraction
N/A not tested