Table 1.
Fusarium Toxins | Corn | Wheat | Barley | |||||||
---|---|---|---|---|---|---|---|---|---|---|
Linearity (r) (a) | Repeatability (%) (b) | Recovery (%) (c) | Linearity (r) | Repeatability (%) | Recovery (%) | Linearity (r) | Repeatability (%) | Recovery (%) | ||
Trichothecenes | NIV | 0.9997 | 2.1 | 76 | 0.9999 | 5.4 | 71 | 0.9996 | 5.1 | 78 |
FUX | 0.9995 | 4.4 | 87 | 0.9998 | 6.2 | 93 | 0.9995 | 7.8 | 102 | |
DON | 0.9993 | 4.2 | 80 | 0.9996 | 6.0 | 89 | 0.9968 | 4.6 | 82 | |
3-ADON | 0.9995 | 5.7 | 92 | 0.9992 | 5.6 | 89 | 0.9978 | 5.8 | 88 | |
15-ADON | 0.9989 | 2.4 | 95 | 0.9990 | 5.0 | 99 | 0.9982 | 6.8 | 96 | |
HT-2 | 0.9999 | 1.4 | 98 | 0.9998 | 1.0 | 101 | 0.9991 | 3.4 | 98 | |
T-2 | 0.9998 | 0.9 | 93 | 0.9994 | 1.7 | 95 | 0.9989 | 1.0 | 94 | |
NEO | 0.9986 | 4.7 | 98 | 0.9987 | 2.9 | 99 | 0.9964 | 7.0 | 100 | |
DAS | 0.9989 | 1.0 | 97 | 0.9979 | 1.5 | 97 | 0.9967 | 2.5 | 97 | |
Fumonisins | FB1 | 0.9999 | 1.6 | 96 | 0.9992 | 2.7 | 85 | 0.9998 | 2.6 | 93 |
FB2 | 0.9994 | 2.4 | 102 | 0.9985 | 3.8 | 91 | 0.9991 | 3.6 | 94 | |
FB3 | 0.9998 | 0.8 | 104 | 0.9998 | 3.4 | 93 | 0.9997 | 3.1 | 94 | |
FA1 | 0.9991 | 1.5 | 100 | 0.9997 | 2.3 | 97 | 0.9997 | 1.6 | 96 | |
FA2 | 0.9999 | 11.9 | 93 | 0.9999 | 6.7 | 106 | 0.9986 | 14.7 | 98 | |
FA3 | 0.9999 | 2.6 | 97 | 0.9996 | 2.6 | 97 | 0.9992 | 2.0 | 97 | |
Zearalenone-group | ZEN | 0.9998 | 3.4 | 82 | 0.9995 | 4.0 | 90 | 0.9997 | 7.3 | 84 |
α-ZEL | 0.9998 | 6.1 | 86 | 0.9994 | 2.4 | 91 | 0.9979 | 4.3 | 79 | |
β-ZEL | 0.9993 | 3.1 | 95 | 0.9997 | 5.6 | 84 | 0.9988 | 7.6 | 92 | |
α-ZAL | 0.9998 | 2.7 | 78 | 0.9998 | 6.4 | 97 | 0.9984 | 12.4 | 82 | |
β-ZAL | 0.9990 | 6.8 | 86 | 0.9999 | 4.1 | 99 | 0.9984 | 6.2 | 78 |
(a) Concentration range of linearity, 5–5000 μg/kg; (b) n = 5, The samples were spiked with 100 μg/kg; (c) n = 1, The samples were spiked with 100 μg/kg. Abbreviations: NIV, nivalenol; FUX, fusarenon-X; DON, deoxynivalenol, 3-ADON, 3-acetyl deoxynivalenol; 15-ADON, 15-acetyl deoxynivalenol; HT-2, HT-2 toxin; T-2, T-2 toxin; NEO, neosolaniol; DAS, diacetoxyscirpenol; FB1, fumonisin B1; FB2, fumonisin B2; FB3, fumonisin B3; FA1, fumonisin A1; FA2, fumonisin A2; FA3, fumonisin A3; ZEN, zearalenone; α-ZEL, α-zearalenol; β-ZEL, β-zearalenol; α-ZAL, α-zearalanol; and β-ZAL, β-zearalanol.