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. 2015 May 14;7(5):1664–1682. doi: 10.3390/toxins7051664

Table 1.

Performance of the method.

Fusarium Toxins Corn Wheat Barley
Linearity (r) (a) Repeatability (%) (b) Recovery (%) (c) Linearity (r) Repeatability (%) Recovery (%) Linearity (r) Repeatability (%) Recovery (%)
Trichothecenes NIV 0.9997 2.1 76 0.9999 5.4 71 0.9996 5.1 78
FUX 0.9995 4.4 87 0.9998 6.2 93 0.9995 7.8 102
DON 0.9993 4.2 80 0.9996 6.0 89 0.9968 4.6 82
3-ADON 0.9995 5.7 92 0.9992 5.6 89 0.9978 5.8 88
15-ADON 0.9989 2.4 95 0.9990 5.0 99 0.9982 6.8 96
HT-2 0.9999 1.4 98 0.9998 1.0 101 0.9991 3.4 98
T-2 0.9998 0.9 93 0.9994 1.7 95 0.9989 1.0 94
NEO 0.9986 4.7 98 0.9987 2.9 99 0.9964 7.0 100
DAS 0.9989 1.0 97 0.9979 1.5 97 0.9967 2.5 97
Fumonisins FB1 0.9999 1.6 96 0.9992 2.7 85 0.9998 2.6 93
FB2 0.9994 2.4 102 0.9985 3.8 91 0.9991 3.6 94
FB3 0.9998 0.8 104 0.9998 3.4 93 0.9997 3.1 94
FA1 0.9991 1.5 100 0.9997 2.3 97 0.9997 1.6 96
FA2 0.9999 11.9 93 0.9999 6.7 106 0.9986 14.7 98
FA3 0.9999 2.6 97 0.9996 2.6 97 0.9992 2.0 97
Zearalenone-group ZEN 0.9998 3.4 82 0.9995 4.0 90 0.9997 7.3 84
α-ZEL 0.9998 6.1 86 0.9994 2.4 91 0.9979 4.3 79
β-ZEL 0.9993 3.1 95 0.9997 5.6 84 0.9988 7.6 92
α-ZAL 0.9998 2.7 78 0.9998 6.4 97 0.9984 12.4 82
β-ZAL 0.9990 6.8 86 0.9999 4.1 99 0.9984 6.2 78

(a) Concentration range of linearity, 5–5000 μg/kg; (b) n = 5, The samples were spiked with 100 μg/kg; (c) n = 1, The samples were spiked with 100 μg/kg. Abbreviations: NIV, nivalenol; FUX, fusarenon-X; DON, deoxynivalenol, 3-ADON, 3-acetyl deoxynivalenol; 15-ADON, 15-acetyl deoxynivalenol; HT-2, HT-2 toxin; T-2, T-2 toxin; NEO, neosolaniol; DAS, diacetoxyscirpenol; FB1, fumonisin B1; FB2, fumonisin B2; FB3, fumonisin B3; FA1, fumonisin A1; FA2, fumonisin A2; FA3, fumonisin A3; ZEN, zearalenone; α-ZEL, α-zearalenol; β-ZEL, β-zearalenol; α-ZAL, α-zearalanol; and β-ZAL, β-zearalanol.