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. 2015 May 20;7(5):1779–1807. doi: 10.3390/toxins7051779

Table 7.

Sampling data and analysis results of random routine shellfish samples obtained in June–July 2014.

Sampling Data MBA (Yasumoto1978) LC-MS/MS
Year Sample Code Date of Collection Regional Unit Site Species Result (24 h) Symptomatology Tissue Tested TTX (μg/kg) 4-epi-TTX (μg/kg) 4,9-anhydro-TTX (μg/kg)
2014 2303/2014 23 June 2014 Chalkidiki X2: South Strymonikos Gulf—Olympiada Mussels Negative (− − −) 3/3 mice with diarrhea HP/WF <LOQ ND ND
2014 272/2014 30 June 2014 Thessaloniki Kymina Mussels Negative (− − −) None HP/WF ND ND ND
2014 2313/2014 30 June 2014 Dytiki Attiki/ Megara Drepano Mussels Negative (− − −) 3/3 mice with bad clinical condition and diarrhea HP ND ND ND
2014 2315/2014 30 June 2014 Dytiki Attiki/ Megara Neraki Mussels Negative (− − −) None HP/WF ND ND ND
2014 1303/2014 01 July 2014 Kavala Keramoti Mussels Negative (− − −) None HP/WF <LOQ ND ND
2014 2323/2014 01 July 2014 Serres S1: Nea Kerdyllia Mussels Negative (− − −) None HP/WF <LOQ ND ND
2014 283/2014 07 July 2014 Thessaloniki Kymina Mussels Negative (− − −) 1/3 mice with mild diarrhea HP/WF ND ND ND
2014 2332/2014 07 July 2014 Dytiki Attiki/ Megara Drepano Mussels Negative (− − −) 3/3 mice with bad clinical condition HP ND ND ND
2014 2334/2014 07 July 2014 Dytiki Attiki/ Megara Neraki Mussels Negative (− − −) None HP/WF ND ND ND
2014 2337/2014 07 July 2014 Chalkidiki X2: South Strymonikos Gulf—Olympiada Mussels Negative (− − −) 1/3 mice with bad clinical condition HP <LOQ ND ND
2014 1307/2014 08 July 2014 Kavala Keramoti Mussels Negative (− − −) None HP ND ND ND
2014 2342/2014 08 July 2014 Serres S1: Nea Kerdyllia Mussels Negative (− − −) 1/3 mice with diarrhea HP ND ND ND
2014 297/2014 14 July 2014 Thessaloniki Kymina Mussels Negative (− − −) 1/3 mice with diarrhea, 2/3 mild diarrhea HP ND ND ND
2014 1311/2014 15 July 2014 Kavala Keramoti Mussels Negative (− − −) 1/3 mice with bad clinical condition HP ND ND ND
2014 2360/2014 15 July 2014 Dytiki Attiki/ Megara Drepano Venus clams Negative (− + −) 1/3 mice dead in 1:05 h, 1/3 diarrhea HP/WF ND ND ND
2014 2368/2014 15 July 2014 Serres S1: Nea Kerdyllia Mussels Negative (− − −) None HP/WF ND ND ND