Table 2. Data collection and refinement statistics.
| Crystal form | Trigonal | Orthorhombic | Hexagonal | |
|---|---|---|---|---|
| (treatment) | - | Wash I | Wash II | - |
| Data collection | ||||
| Space group | P3221 | P212121 | P212121 | P6122 |
| Cell dimensions | ||||
| a, b, c (Å) | 51.7,51.7, 84.7 | 57.3, 59.6 86.7 | 56.7, 59.7, 88.1 | 137.9, 137.9, 154.4 |
| Resolution (Å) | 30.8–1.20 (1.27–1.20)* | 37.3–1.75 (1.86–1.75)* | 37.2–1.75 (1.86–1.75)* | 39.0–2.90 (3.07–2.90)* |
| R merge | 5.7 (74.4) | 4.8 (68.2) | 6.6 (47.6) | 9.9 (53.2) |
| I/σI | 11.85 (1.78) | 16.98 (1.90) | 9.79 (2.16) | 10.53 (2.22) |
| Completeness (%) | 99.7 (99.3) | 99.7 (98.7) | 97.7 (96.5) | 99.1 (98.3) |
| Redundancy | 3.91 (3.69) | 4.23 (4.23) | 2.86 (2.79) | 2.97 (2.95) |
| Refinement | ||||
| Resolution (Å) | 30.8–1.20 | 37.3–1.75 | 37.2–1.75 | 39.0–2.90 |
| No. reflections | 39531 | 29087 | 28637 | 18776 |
| R work / R free | 0.13 / 0.16 | 0.17 / 0.21 | 0.15 / 0.19 | 0.17 / 0.22 |
| # chains / AU | 1 | 3 | 3 | 4 |
| PDB code | 5AMH | 5AMI | 5AMJ | 5AMK |
*Highest resolution shell is shown in parenthesis.