Table 2. Refinement statistics.
| Lysozyme | |||||
|---|---|---|---|---|---|
| Data | 30min Control | Control 1 | Vacuum Thick | Vacuum Thin | Proteinase K |
| Resolution range () | 201.80 | 201.80 | 201.80 | 202.8 | 201.91 |
| Reflections used for refinement (all) | 10216 | 10084 | 9703 | 2733 | 17993 |
| Reflections used for R free | 988 | 983 | 949 | 123 | 1030 |
| R cryst † | 18.9 | 19.5 | 17.4 | 24.9 | 14.1 |
| R free | 23.8 | 23.1 | 20.7 | 30.9 | 18.7 |
| R.m.s. deviation for bonds () | 0.023 | 0.022 | 0.024 | 0.012 | 0.025 |
| R.m.s. deviation for angles () | 1.811 | 1.832 | 1.961 | 1.585 | 1.871 |
| Residues in most favoured region (%) | 87.6 | 86.7 | 85.8 | 71.65 | 89.8 |
| Residues in additional allowed region (%) | 12.4 | 13.3 | 14.2 | 14.96 | 9.8 |
| Residues in generously allowed regions (%) | 0 | 0 | 0 | 13.39 | 0.4 |
| Disallowed region (%) | 0 | 0 | 0 | 0 | 0 |
†
Statistics are based on PROCHECK (Laskowski et al., 1993 ▶).