| Crystal data |
| Chemical formula |
[Ge(CH3)3(C7H5O2)] |
|
M
r
|
238.80 |
| Crystal system, space group |
Triclinic, P
|
| Temperature (K) |
173 |
|
a, b, c () |
6.3560(4), 12.3927(6), 14.2084(7) |
| , , () |
96.348(4), 92.846(4), 93.246(4) |
|
V (3) |
1108.76(10) |
|
Z
|
4 |
| Radiation type |
Mo K
|
| (mm1) |
2.73 |
| Crystal size (mm) |
0.08 0.08 0.02 |
| |
| Data collection |
| Diffractometer |
Agilent Xcalibur Sapphire3 |
| Absorption correction |
Multi-scan (CrysAlis PRO; Agilent, 2014 ▸) |
|
T
min, T
max
|
0.794, 1.000 |
| No. of measured, independent and observed [I > 2(I)] reflections |
15667, 4781, 3261 |
|
R
int
|
0.044 |
| (sin /)max (1) |
0.639 |
| |
| Refinement |
|
R[F
2 > 2(F
2)], wR(F
2), S
|
0.036, 0.083, 1.02 |
| No. of reflections |
4781 |
| No. of parameters |
249 |
| H-atom treatment |
H atoms treated by a mixture of independent and constrained refinement |
|
max, min (e 3) |
0.54, 0.31 |
