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. 2015 May 23;71(Pt 6):698–701. doi: 10.1107/S2056989015009664

Table 2. Experimental details.

Crystal data
Chemical formula [Ag2(CN)3(C9H8N2)2]
M r 582.15
Crystal system, space group Monoclinic, P21/c
Temperature (K) 293
a, b, c () 13.5449(7), 6.9385(3), 22.3824(11)
() 94.767(2)
V (3) 2096.25(17)
Z 4
Radiation type Mo K
(mm1) 1.89
Crystal size (mm) 0.27 0.23 0.18
 
Data collection
Diffractometer Bruker APEXII CCD
Absorption correction Multi-scan (SADABS; Sheldrick, 2003)
T min, T max 0.615, 0.754
No. of measured, independent and observed [I > 2(I)] reflections 27103, 7113, 5226
R int 0.021
(sin /)max (1) 0.750
 
Refinement
R[F 2 > 2(F 2)], wR(F 2), S 0.034, 0.088, 1.02
No. of reflections 7113
No. of parameters 283
H-atom treatment H atoms treated by a mixture of independent and constrained refinement
max, min (e 3) 1.70, 0.56

Computer programs: APEX2 and SAINT (Bruker, 2009), SHELXS2014/7 (Sheldrick, 2008), SHELXL2014/7 (Sheldrick, 2015) and Mercury (Macrae et al., 2008).