| Crystal data |
| Chemical formula |
K5[H2PtV9O28]9H2O |
|
M
r
|
1461.21 |
| Crystal system, space group |
Triclinic, P
|
| Temperature (K) |
298 |
|
a, b, c () |
10.1663(7), 12.8350(7), 13.615(2) |
| , , () |
103.734(5), 106.193(6), 92.480(4) |
|
V (3) |
1645.8(3) |
|
Z
|
2 |
| Radiation type |
Mo K
|
| (mm1) |
7.42 |
| Crystal size (mm) |
0.21 0.19 0.17 |
| |
| Data collection |
| Diffractometer |
Stoe Stadi4 |
| Absorption correction |
Empirical (using intensity measurements) (X-SHAPE; Stoe Cie,1996 ▸) |
|
T
min, T
max
|
0.301, 0.378 |
| No. of measured, independent and observed [I > 2(I)] reflections |
6797, 6797, 6242 |
| (sin /)max (1) |
0.628 |
| |
| Refinement |
|
R[F
2 > 2(F
2)], wR(F
2), S
|
0.028, 0.066, 1.10 |
| No. of reflections |
6797 |
| No. of parameters |
526 |
| No. of restraints |
25 |
| H-atom treatment |
H atoms treated by a mixture of independent and constrained refinement |
|
max, min (e 3) |
1.30, 1.46 |
