Table 2. Experimental details.
| Crystal data | |
| Chemical formula | C10H15ClNS+Cl |
| M r | 252.19 |
| Crystal system, space group | Monoclinic, P21/n |
| Temperature (K) | 298 |
| a, b, c () | 6.5717(10), 11.8058(17), 16.201(2) |
| () | 97.374(3) |
| V (3) | 1246.5(3) |
| Z | 4 |
| Radiation type | Mo K |
| (mm1) | 0.65 |
| Crystal size (mm) | 0.28 0.24 0.20 |
| Data collection | |
| Diffractometer | Bruker APEXII CCD |
| Absorption correction | Multi-scan (SADABS; Bruker, 2013 ▸) |
| T min, T max | 0.839, 0.881 |
| No. of measured, independent and observed [I > 2(I)] reflections | 9002, 2255, 1584 |
| R int | 0.100 |
| (sin /)max (1) | 0.600 |
| Refinement | |
| R[F 2 > 2(F 2)], wR(F 2), S | 0.065, 0.158, 1.04 |
| No. of reflections | 2255 |
| No. of parameters | 128 |
| H-atom treatment | H-atom parameters constrained |
| max, min (e 3) | 0.50, 0.23 |