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. 2015 May 13;71(Pt 6):618–620. doi: 10.1107/S2056989015008701
Refinement on F2 Primary atom site location: structure-invariant direct methods
Least-squares matrix: full Secondary atom site location: difference Fourier map
R[F2 > 2σ(F2)] = 0.048 Hydrogen site location: inferred from neighbouring sites
wR(F2) = 0.139 H-atom parameters constrained
S = 1.05 w = 1/[σ2(Fo2) + (0.0667P)2 + 0.2293P] where P = (Fo2 + 2Fc2)/3
6718 reflections (Δ/σ)max < 0.001
301 parameters Δρmax = 0.40 e Å3
0 restraints Δρmin = −0.40 e Å3