| Crystal data |
| Chemical formula |
C10H10INO |
|
M
r
|
287.09 |
| Crystal system, space group |
Orthorhombic, P212121
|
| Temperature (K) |
295 |
|
a, b, c () |
4.4622(1), 8.2664(2), 27.4400(5) |
|
V (3) |
1012.16(4) |
|
Z
|
4 |
| Radiation type |
Mo K
|
| (mm1) |
3.12 |
| Crystal size (mm) |
0.42 0.32 0.16 |
| |
| Data collection |
| Diffractometer |
Bruker APEXII CCD |
| Absorption correction |
Multi-scan (SADABS; Bruker, 2005 ▸) |
|
T
min, T
max
|
0.354, 0.635 |
| No. of measured, independent and observed [I > 2(I)] reflections |
12175, 2938, 2878 |
|
R
int
|
0.020 |
| (sin /)max (1) |
0.704 |
| |
| Refinement |
|
R[F
2 > 2(F
2)], wR(F
2), S
|
0.021, 0.050, 1.21 |
| No. of reflections |
2938 |
| No. of parameters |
148 |
| H-atom treatment |
H atoms treated by a mixture of independent and constrained refinement |
|
max, min (e 3) |
0.47, 0.69 |
| Absolute structure |
Flack (1983 ▸), 1183 Friedel pairs |
| Absolute structure parameter |
0.02(2) |
