Table 2. Experimental details.
| Crystal data | |
| Chemical formula | Ba(ClO4)2 |
| M r | 336.23 |
| Crystal system, space group | Orthorhombic, F d d d |
| Temperature (K) | 298 |
| a, b, c () | 14.304(9), 11.688(7), 7.2857(4) |
| V (3) | 1218.1(11) |
| Z | 8 |
| Radiation type | Cu K 1, = 1.54059 |
| Specimen shape, size (mm) | Flat sheet, 20 20 |
| Data collection | |
| Diffractometer | PANalytical Empyrean |
| Specimen mounting | Packed powder |
| Data collection mode | Reflection |
| Scan method | Step |
| 2 values () | 2min = 14.992 2max = 129.964 2step = 0.026 |
| Refinement | |
| R factors and goodness of fit | R p = 0.041, R wp = 0.060, R exp = 0.045, R(F 2) = 0.05733, 2 = 1.769 |
| No. of data points | 4423 |
| No. of parameters | 25 |