Table 2. Experimental details.
| Crystal data | |
| Chemical formula | [Cr(NCS)2(C2H8N2)2]ClO4 |
| M r | 387.82 |
| Crystal system, space group | Monoclinic, C2/c |
| Temperature (K) | 260 |
| a, b, c () | 15.599(3), 7.4440(15), 13.792(3) |
| () | 105.83(3) |
| V (3) | 1540.8(6) |
| Z | 4 |
| Radiation type | Synchrotron, = 0.630 |
| (mm1) | 0.86 |
| Crystal size (mm) | 0.14 0.13 0.13 |
| Data collection | |
| Diffractometer | ADSC Q210 CCD area detector |
| Absorption correction | Empirical (using intensity measurements) (HKL3000sm SCALEAPCK; Otwinowski Minor, 1997 ▸) |
| T min, T max | 0.893, 0.897 |
| No. of measured, independent and observed [I > 2(I)] reflections | 8172, 2121, 2019 |
| R int | 0.015 |
| (sin /)max (1) | 0.696 |
| Refinement | |
| R[F 2 > 2(F 2)], wR(F 2), S | 0.060, 0.178, 1.09 |
| No. of reflections | 2121 |
| No. of parameters | 140 |
| H-atom treatment | H-atom parameters constrained |
| max, min (e 3) | 0.74, 1.12 |