| Crystal data |
| Chemical formula |
C14H13ClN2O2S |
|
M
r
|
308.77 |
| Crystal system, space group |
Triclinic, P
|
| Temperature (K) |
296 |
|
a, b, c () |
6.5661(10), 10.2595(18), 11.3490(19) |
| , , () |
69.101(7), 88.219(7), 77.238(7) |
|
V (3) |
695.6(2) |
|
Z
|
2 |
| Radiation type |
Mo K
|
| (mm1) |
0.43 |
| Crystal size (mm) |
0.23 0.18 0.16 |
| |
| Data collection |
| Diffractometer |
Bruker APEXII CCD |
| Absorption correction |
Multi-scan (SADABS; Bruker, 2013 ▸) |
|
T
min, T
max
|
0.912, 0.934 |
| No. of measured, independent and observed [I > 2(I)] reflections |
9865, 2454, 1980 |
|
R
int
|
0.053 |
| (sin /)max (1) |
0.595 |
| |
| Refinement |
|
R[F
2 > 2(F
2)], wR(F
2), S
|
0.050, 0.146, 1.09 |
| No. of reflections |
2454 |
| No. of parameters |
181 |
| H-atom treatment |
H-atom parameters constrained |
|
max, min (e 3) |
0.59, 0.43 |