Table 2. Experimental details.
| Crystal data | |
| Chemical formula | C14H13NO2 |
| M r | 227.25 |
| Crystal system, space group | Monoclinic, P c |
| Temperature (K) | 100 |
| a, b, c () | 8.0357(3), 5.5554(2), 12.8733(5) |
| () | 101.312(1) |
| V (3) | 563.52(4) |
| Z | 2 |
| Radiation type | Mo K |
| (mm1) | 0.09 |
| Crystal size (mm) | 0.55 0.48 0.41 |
| Data collection | |
| Diffractometer | Bruker APEXII D8 Venture |
| Absorption correction | Multi-scan (SADABS; Bruker, 2009 ▸) |
| T min, T max | 0.953, 0.964 |
| No. of measured, independent and observed [I > 2(I)] reflections | 26314, 3449, 3414 |
| R int | 0.023 |
| (sin /)max (1) | 0.715 |
| Refinement | |
| R[F 2 > 2(F 2)], wR(F 2), S | 0.037, 0.100, 1.09 |
| No. of reflections | 3449 |
| No. of parameters | 160 |
| No. of restraints | 2 |
| H-atom treatment | H atoms treated by a mixture of independent and constrained refinement |
| max, min (e 3) | 0.37, 0.28 |