Skip to main content
. 2015 May 20;71(Pt 6):644–646. doi: 10.1107/S2056989015009196

Table 2. Experimental details.

Crystal data
Chemical formula [PtCl2(C5H11N)(C6H6N2O2)]
M r 489.27
Crystal system, space group Monoclinic, C2/c
Temperature (K) 100
a, b, c () 15.8763(11), 18.5394(11), 10.8707(6)
() 103.119(7)
V (3) 3116.1(3)
Z 8
Radiation type Mo K
(mm1) 9.35
Crystal size (mm) 0.35 0.15 0.1
 
Data collection
Diffractometer Agilent SuperNova (single source at offset, Eos detector)
Absorption correction Multi-scan (CrysAlis PRO; Agilent, 2012)
T min, T max 0.538, 1.000
No. of measured, independent and observed [I > 2(I)] reflections 8156, 3109, 2713
R int 0.044
(sin /)max (1) 0.625
 
Refinement
R[F 2 > 2(F 2)], wR(F 2), S 0.032, 0.072, 1.10
No. of reflections 3109
No. of parameters 172
H-atom treatment H-atom parameters constrained
max, min (e 3) 2.75, 1.82

Computer programs: CrysAlis PRO (Agilent, 2012), SHELXS97 and SHELXL97 (Sheldrick, 2008) and OLEX2 (Dolomanov et al., 2009).