Table 1.
Sample No. | L (mm) | A (mm2) | T (°C) | έ × 104 (s−1) | Δε × 103 | E (MPa) | R 2 | Failure stress (MPa) | |
---|---|---|---|---|---|---|---|---|---|
PEG400 | 1 | 35.00 | 8.84 | −149.3 | 0.73 | 0.07 | 2279 | 0.999 | 6.99 |
2 | 31.66 | 7.54 | −145.0 | 0.80 | 3.60 | 2475 | 0.999 | 11.21 | |
3 | 26.48 | 8.04 | −139.8 | 0.96 | 1.91 | 2006 | 0.999 | 9.67 | |
4 | 26.00 | 7.04 | −143.0 | 0.98 | 2.34 | 2479 | 1.000 | 12.58 | |
5 | 30.42 | 8.84 | −139.8 | 0.84 | 2.41 | 2001 | 0.999 | 12.44 | |
6 | 23.26 | 8.27 | −143.9 | 1.09 | 6.21 | 2426 | 0.999 | 15.91 | |
Average | 28.80 | 8.10 | −143.46 | 0.90 | 2.07 | 2248 ± 224 a | 0.999 | 10.58 ± 3.01 a | |
7.05 M DMSO | 1 | 28.00 | 9.40 | −150.0 | 0.91 | 6.35 | 922 | 0.999 | 7.38 |
2 | 25.70 | 10.33 | −147.5 | 0.99 | 5.58 | 950 | 0.999 | 9.80 | |
3 | 31.34 | 10.72 | −153.9 | 0.81 | 6.88 | 1011 | 0.999 | 12.22 | |
4 | 25.93 | 8.98 | −142.9 | 0.98 | 10.30 | 1495 | 1.000 | 15.68 | |
5 | 31.21 | 6.78 | −167.7 | 0.81 | 1.83 | 2955 | 0.999 | 14.81 | |
6 | 21.68 | 9.44 | −146.2 | 1.17 | 7.88 | 1839 | 0.999 | 13.89 | |
7 | 30.48 | 11.30 | −148.6 | 0.83 | 4.99 | 2240 | 0.999 | N/A | |
8 | 24.67 | 7.26 | −163.1 | 1.03 | 4.61 | 2700 | 0.999 | 18.01 | |
9 | 22.71 | 12.50 | −138.2 | 1.12 | 8.15 | 1631 | 0.999 | 12.44 | |
Average | 28.44 | 9.24 | −152.39 | 0.90 | 6.19 | 2143 ± 754 a | 0.999 | 11.98 ± 3.36 a | |
1,3-CHD | 1 | 27.39 | 10.49 | −151.0 | 0.93 | 2.32 | 1480 | 1.000 | 9.59 |
2 | 22.46 | 8.03 | −142.8 | 1.11 | 7.03 | 2080 | 0.999 | 17.96 | |
3 | 24.48 | 8.11 | −150.0 | 1.04 | 2.69 | 2310 | 1.000 | 10.07 | |
4 | 27.19 | 8.31 | −144.3 | 0.93 | 3.06 | 1777 | 0.999 | 6.65 | |
5 | 25.63 | 8.66 | −145.5 | 0.99 | 2.46 | 2448 | 0.999 | 15.92 | |
Average | 25.43 | 8.72 | −146.7 | 1.00 | 3.51 | 2019 ± 394 a | 0.999 | 12.04 ± 4.72 a | |
2,3BD | 1 | 21.31 | 7.21 | −148.3 | 1.19 | 2.14 | 2940 | 0.999 | 12.83 |
2 | 28.31 | 10.71 | −143.3 | 0.90 | 1.77 | 2868 | 0.999 | 10.05 | |
3 | 29.07 | 8.80 | −146.0 | 0.87 | 1.66 | 3012 | 1.000 | 19.72 | |
4 | 22.68 | 6.93 | −153.0 | 1.12 | 3.95 | 2811 | 0.999 | 18.68 | |
5 | 19.35 | 8.15 | −144.2 | 1.31 | 5.10 | 2062 | 0.999 | 15.64 | |
6 | 24.24 | 9.79 | −147.0 | 1.04 | 5.27 | 1688 | 0.999 | 14.65 | |
7 | 24.26 | 8.67 | −141.0 | 1.05 | 5.22 | 2298 | 0.999 | 19.32 | |
8 | 19.07 | 8.62 | −151.7 | 1.33 | 1.92 | 1675 | 0.999 | 12.19 | |
9 | 24.01 | 8.52 | −149.8 | 1.06 | 7.38 | 2416 | 0.999 | 16.46 | |
Average | 23.59 | 8.60 | −147.14 | 1.10 | 3.82 | 2419 ± 525 a | 0.999 | 15.50 ± 3.39 a | |
Frozen | 1 | 23.29 | 9.79 | −146.1 | 1.09 | 4.84 | 1226 | 0.996 | 5.25 |
Standard deviation