Table 1. Data collection and refinement statistics.
| pCBL-B–UbcH5B–Ub–ZAP-70 peptide | |
|---|---|
| Data collection | |
| Space group | P1211 |
| Cell dimensions | |
| a, b, c (Å) | 95.0, 131.8, 122.0 |
| αβγ(°) | 90.0, 91.9, 90.0 |
| Resolution (Å) | 30.54–2.21(2.27–2.21)a |
| Rmerge | 0.058(0.688) |
| I/σI | 14.2(2.1) |
| Completeness (%) | 99.6(99.9) |
| Redundancy | 3.4(3.5) |
| Refinement | |
| Resolution (Å) | 30.5–2.21 |
| No. reflections | 149230 |
| Rwork/Rfree | 0.175/0.211 |
| No. atoms | |
| Protein | 19758 |
| Ligand/ion | 12 |
| Water | 776 |
| B factors | |
| Protein | 48.1 |
| Ligand/ion | 44.1 |
| Water | 41.0 |
| r.m.s. deviations | |
| Bond lengths (Å) | 0.004 |
| Bond angles (°) | 0.811 |
a
Values in parentheses are for highest-resolution shell.