Tab. 3.
Repeatability and intermediate precision which compose the precision parameter of the analytical method proposed
| Sample | Repeatability | Intermediate Precision | Repeatability | Intermediate Precision |
|---|---|---|---|---|
| γ-CyD : FP complex + PVA 0.1% (mg/ml) | γ-CyD : FP complex + PEG 0.5% (mg/ml) | |||
| 1 | 0.0684 | 0.0684 | 0.0601 | 0.0601 |
| 2 | 0.0719 | 0.0719 | 0.0622 | 0.0622 |
| 3 | 0.0690 | 0.0690 | 0.0628 | 0.0628 |
| 4 | 0.0707 | 0.0707 | 0.0653 | 0.0653 |
| 5 | 0.0645 | 0.0645 | 0.0581 | 0.0581 |
| 6 | 0.0678 | 0.0678 | 0.0621 | 0.0621 |
| 7 | 0.0766 | 0.0669 | ||
| 8 | 0.0817 | 0.0647 | ||
| 9 | 0.0759 | 0.0703 | ||
| 10 | 0.0818 | 0.0683 | ||
| 11 | 0.0641 | 0.0653 | ||
| 12 | 0.0740 | 0.0616 | ||
| Average | 0.0687 | 0.0722 | 0.0618 | 0.0640 |
| %RSD | 3.72 | 8.25 | 3.98 | 5.22 |
Samples 1–6 were performed by analyst 1 in Day 1 and samples 7–12 were performed by analyst 2 in Day 2.