Tab. 1.
9 | 11 | 9 | 11 | |||||
---|---|---|---|---|---|---|---|---|
H/C | (ppm) | J(Hz) | M | (ppm) | J(Hz) | M | (ppm) | (ppm) |
1 | 172.2 | 175.8 | ||||||
2 | 5.28 | 2.4 | d | 4.25 | 2.0 | d | 73.6 | 72.3 |
3 | 4.20 | 2.4, 5.0, 9.0 | ddd | 4.22 | 2.0, 6.0, 8.0 | ddd | 72.7 | 72.2 |
4a | 3.63 | 6.0, -11.0 | dd | 4.27 | 8.0, -11.0 | dd | 63.1 | 65.9 |
4b | 3.61 | 8.0, -11.0 | dd | 4.26 | 6.0, -11.0 | dd | ||
1’ | 127.8 | 127.2 | ||||||
2’ | 7.08 | 2.1 | d | 7.46 | 8.5, 2.3 | dd | 115.3 | 131.2 |
3’ | 6.80 | 8.5, 2.3 | dd | 146.8 | 116.8 | |||
4’ | 149.7 | 161.2 | ||||||
5’ | 6.79 | 8.2 | d | 6.80 | 8.5, 2.3 | dd | 116.5 | 116.8 |
6’ | 6.79 | 2.1, 8.2 | dd | 7.46 | 8.5, 2.3 | dd | 123.1 | 131.2 |
7’ | 7.68 | 15.8 | d | 7.64 | 16.0 | d | 147.9 | 146.8 |
8’ | 6.37 | 15.8 | d | 6.35 | 16.0 | d | 114.4 | 115.0 |
9’ | 168.5 | 169.0 |