Skip to main content
. Author manuscript; available in PMC: 2015 Jun 25.
Published in final edited form as: Aerosol Air Qual Res. 2014 Dec;14(7):1939–1949. doi: 10.4209/aaqr.2013.10.0312

Table 2.

Extraction efficiency under designed extraction conditions.

Test Extraction condition Extraction buffer %recovery of Cr(VI) (Mean ± SD, N = 3)
PbCrO4 BaCrO4
1 15 min Ramping to 95°C and holding for 1 hr, pressure less than 220 psi 3% Na2CO3-2% NaOH 95.0 ± 5.5% 78.0 ± 3.1%
2 15 min Ramping to 60°C and holding for 1 hr, pressure less than 200 psi 43.7 ± 8.3% 16.5 ± 5.4%
3 15 min Ramping to 95°C and holding for 40 min, pressure less than 200 psi 81.3 ± 1.8% 42.3 ± 0.5%

4 15 min Ramping to 95°C and holding for 1 hr, pressure less than 220 psi 1:2.5 diluted
3% Na2CO3-2% NaOH
62.8 ± 6.0% 57.2 ± 8.8%
5 1:5 diluted
3% Na2CO3-2% NaOH
55.1 ± 7.0% 39.5 ± 6.2%