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. Author manuscript; available in PMC: 2016 Aug 1.
Published in final edited form as: Nucl Med Biol. 2015 Apr 20;42(8):673–684. doi: 10.1016/j.nucmedbio.2015.04.005

Scheme 1.

Scheme 1

Synthesis of tosylate precursor of FPOIBG and FPOBBG.

a) (3-Bromopropoxy)-(tert-butyl)-dimethylsilane, Kl, K2CO3, Acetonitrile b) NBS, benzoyl peroxide, Dichloromethane c) (Boc)2guanidine, Pot. tert-butoxide, THF d) TBAF/THF e) 1-Tosyl-3-methyl imidazolinium triflate, 1-methyl imidazole, THF