Table 1.
| ||
---|---|---|
entry | product | yield (%)[b] |
1 |
2a |
40 |
2 |
2b |
39 |
3 |
2c |
40 |
4 |
2d |
41 |
5 |
2e |
45 |
Reaction conditions: phenols 1 (10 mmol), sulfuryl chloride (22 mmol), NaN3 (30 mmol).
Isolated yields.
| ||
---|---|---|
entry | product | yield (%)[b] |
1 |
2a |
40 |
2 |
2b |
39 |
3 |
2c |
40 |
4 |
2d |
41 |
5 |
2e |
45 |
Reaction conditions: phenols 1 (10 mmol), sulfuryl chloride (22 mmol), NaN3 (30 mmol).
Isolated yields.