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. Author manuscript; available in PMC: 2016 Jun 3.
Published in final edited form as: Tetrahedron Lett. 2015 Jun 3;56(23):3431–3434. doi: 10.1016/j.tetlet.2015.01.186

Table 1.

Preparation of aryloxysulfonyl azides [a]

graphic file with name nihms663034u1.jpg
entry product yield (%)[b]
1 graphic file with name nihms663034t1.jpg
2a
40
2 graphic file with name nihms663034t2.jpg
2b
39
3 graphic file with name nihms663034t3.jpg
2c
40
4 graphic file with name nihms663034t4.jpg
2d
41
5 graphic file with name nihms663034t5.jpg
2e
45
[a]

Reaction conditions: phenols 1 (10 mmol), sulfuryl chloride (22 mmol), NaN3 (30 mmol).

[b]

Isolated yields.