Table 1.
Cross-coupling of phenols and alcohols.
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1/2/PhenoFluor/TMS-imidazole=1.0:2.0:2.0:4.0.
1/2/PhenoFluor/TMS-imidazole=1.5:1.0:1.5:3.0.
1/2/PhenoFluor/TMS-imidazole= 1.0:3.0:3.0:6.0.
TMSNEt2 was used instead of TMS-imidazole.
A yield of 85% was obtained when the reaction was carried out at 80 °C.
Toluene was used as the solvent instead of dioxane.
Bn=benzyl, Bz=benzoyl.