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. 2015 Jul 1;10(7):e0131519. doi: 10.1371/journal.pone.0131519

Fig 3. Synthetic scheme of compounds 23, 24, 33, 34, 35, 38.

Fig 3

Reagents and conditions: i) from 1 for 23, from 5 for 24, from 32 for 33: H2SO4, MeOH, reflux, 1 h; ii) from 32: Py · SO3, DMF dry, 120°C, 25 min; iii) CH3I, anhydrous K2CO3, dry DMF, reflux, 1.5 h; iv) 1N NaOH, EtOH.