Table 1.
Yields of 3 under ultrasound solvent-free conditions
| Entry | Power/W | Time/min | Yielda/% |
|---|---|---|---|
| 1 | 200 | 150 | 38 |
| 2 | 250 | 120 | 41 |
| 3 | 300 | 80 | 46 |
| 4 | 350 | 50 | 54 |
| 5 | 400 | 50 | 54 |
Aniline (10 mmol), α-bromoacetophenone (20 mmol), sodium carbonate (10 mmol), and 2 mol% PEG 400
aIsolated yield