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. 2013 Apr 26;145(1):213–216. doi: 10.1007/s00706-013-0978-7

Table 2.

Effect of the amount of PEG 400 on the synthesis of 3a under ultrasound irradiation

Entry PEG 400/mol% Time/min Yielda/%
1 0 150 11
2 1 90 35
3 2 80 54
4 3 60 71
5 4 50 77
6 5 30 81
7 6 30 82

Aniline (10 mmol), α-bromoacetophenone (20 mmol), sodium carbonate (10 mmol), and 350 W ultrasound

aIsolated yield