Table 2.
Effect of the amount of PEG 400 on the synthesis of 3a under ultrasound irradiation
| Entry | PEG 400/mol% | Time/min | Yielda/% |
|---|---|---|---|
| 1 | 0 | 150 | 11 |
| 2 | 1 | 90 | 35 |
| 3 | 2 | 80 | 54 |
| 4 | 3 | 60 | 71 |
| 5 | 4 | 50 | 77 |
| 6 | 5 | 30 | 81 |
| 7 | 6 | 30 | 82 |
Aniline (10 mmol), α-bromoacetophenone (20 mmol), sodium carbonate (10 mmol), and 350 W ultrasound
aIsolated yield