Table 1.
Variation of the yield of the isolated product resulting from changes to the reaction conditions [see Eq. (1)].
Entry | Deviation from the reaction conditions given in Equation (1) | Yield [%] |
---|---|---|
1 | 10 mol % AgBF4 | 36 |
2 | 1 equiv AgSbF6 | 18 |
3 | 1 equiv AgOAc, AgCN and AgF | <5 |
4 | 10 mol % AgOAc, 1 equiv Bu4NBF4 | <5 |
5 | 10 mol % AgOAc, 1 equiv (tBu)3PHBF4 | 44 |
6 | 1 equiv AgBF4, 1 equiv Selectfluor instead of 1 | <5 |
7 | 1 equiv Zn(BF4)2 | 46 |
8 | 1 equiv Cu(MeCN)4BF4 | 32 |
9 | 1 equiv ZnF2, CuF2 | <5 |
10 | MeOH as solvent | <5 |
11 | toluene as solvent | trace |