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. 2014 Oct 21;53(47):12897–12901. doi: 10.1002/anie.201408812

Table 1.

Variation of the yield of the isolated product resulting from changes to the reaction conditions [see Eq. (1)].

Entry Deviation from the reaction conditions given in Equation (1) Yield [%]
1 10 mol % AgBF4 36
2 1 equiv AgSbF6 18
3 1 equiv AgOAc, AgCN and AgF <5
4 10 mol % AgOAc, 1 equiv Bu4NBF4 <5
5 10 mol % AgOAc, 1 equiv (tBu)3PHBF4 44
6 1 equiv AgBF4, 1 equiv Selectfluor instead of 1 <5
7 1 equiv Zn(BF4)2 46
8 1 equiv Cu(MeCN)4BF4 32
9 1 equiv ZnF2, CuF2 <5
10 MeOH as solvent <5
11 toluene as solvent trace