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. 2015 Jul 16;10(7):e0133075. doi: 10.1371/journal.pone.0133075

Table 1. Signal assignments and relative contents of compounds identified in the 1H NMR spectra of different extracts.

label chemical shift green cultures* chlorotic cultures* compound
AQUEOUS EXTRACT a 1.2, 2.5, 4.15 5 2 β-hydroxy butyric acid
b 3.25 2 0 glycinebetaine
c 1.35 0.7 0.1 lactic acid
d 1.9 2 3 acetic acid
e 3.5–4.0, 5.4 12 0.2 sugars
METHANOLIC EXTRACT d 2.9 1.3 5 acetic acid
e 3.5–4.0 4 0.5 sugars
h 8.55 0.1 1.6 formic acid
i 5.96, 6.16, 8.03, 8.45, 9.35, 9.6 0.8 0 chlorophyll a
j 5.3, 5.4 9 3 unsaturated fatty acids
k 0.9, 1.3 16 17 saturated fatty acids
CHLOROFORMIC EXTRACT k 0.9, 1.3 1.5 1.7 saturated fatty acids
l 1.28, 2.55, 5.26 traces 0.2 poly-β-hydroxy butyric acid

* Intensities were measured relative to the internal standards, Trimethylsilyl Propionic-2,2,3,3,-d4 acid (TMSP) and Tetramethylsilane (TMS).