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. 2015 May 4;21(24):8840–8850. doi: 10.1002/chem.201405994

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© 2015 The Authors. Published by Wiley-VCH Verlag GmbH & Co. KGaA. This is an open access article under the terms of the Creative Commons Attribution-NonCommercial License, which permits use, distribution and reproduction in any medium, provided the original work is properly cited and is not used for commercial purposes.

© 2015 The Authors. Published by Wiley-VCH Verlag GmbH & Co. KGaA. This is an open access article under the terms of the Creative Commons Attribution-NonCommercial License, which permits use, distribution and reproduction in any medium, provided the original work is properly cited and is not used for commercial purposes.

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MAS ¹H NMR data (5 kHz spinning) of hydrated pure DPPC and DPPC/B12 MLV preparations. a) Exemplary quantitative ¹H NMR spectra of a 4:1 mixture obtained by using a recycle delay of 8 s at 20 and 70 °C. b) Integrals of different spectral regions, normalized to 100 % as the total expected signal, as a function of temperature overlaid with scaled DSC traces (right vertical scale) and c) double-quantum (DQ) spinning sideband pattern (10 kHz MAS) for the aromatic B12 resonance of a 4:1 mixture at 75 °C by using the BaBa-xy16 pulse sequence[55] with a recoupling time of 4 rotor periods.