Figure - PMC

Skip to main content

An official website of the United States government

Here's how you know

Here's how you know

Official websites use .gov
A .gov website belongs to an official government organization in the United States.

Secure .gov websites use HTTPS
A lock ( ) or https:// means you've safely connected to the .gov website. Share sensitive information only on official, secure websites.

View full-text article in PMC

. 2014 Jul 14;20(30):9442–9450. doi: 10.1002/chem.201402757

Search in PMC
Search in PubMed
View in NLM Catalog
Add to search

© 2014 The Authors. Published by Wiley-VCH Verlag GmbH & Co. KGaA. This is an open access article under the terms of Creative Commons Attribution NonCommercial-NoDerivs License, which permits use and distribution in any medium, provided the original work is properly cited, the use is non-commercial and no modifications or adaptations are made.

© 2014 The Authors. Published by Wiley-VCH Verlag GmbH & Co. KGaA. This is an open access article under the terms of Creative Commons Attribution NonCommercial-NoDerivs License, which permits use and distribution in any medium, provided the original work is properly cited, the use is non-commercial and no modifications or adaptations are made.

PMC Copyright notice

Schematic of apparatus for continuous high-pressure disilylation. Exemplary conditions for 1,2-bis(trichlorosilyl)decane: Catalyst (n-tetradecyl)tri-n-butylphoshonium chloride; mole ratio decene/trichlorosilane/R₄P⁺Cl⁻ 1:2:0.1; reaction temperature: 180°C; residence time: 2 h; pressure: 23 atm.; yield: 84 %; byproducts: 1-(trichlorosilyl)-2-(dichlorosilyl)decane, trichlorosilyldecane, SiCl₄, H₂SiCl₂.