| Crystal data |
| Chemical formula |
C14H24N2O5S |
|
M
r
|
332.41 |
| Crystal system, space group |
Monoclinic, P21
|
| Temperature (K) |
173 |
|
a, b, c () |
11.509(3), 5.9290(18), 25.751(8) |
| () |
98.307(3) |
|
V (3) |
1738.7(9) |
|
Z
|
4 |
| Radiation type |
Mo K
|
| (mm1) |
0.21 |
| Crystal size (mm) |
0.50 0.15 0.05 |
| |
| Data collection |
| Diffractometer |
Bruker APEXII CCD area detector |
| Absorption correction |
Multi-scan (SADABS; Bruker, 2008 ▸) |
|
T
min, T
max
|
0.88, 0.99 |
| No. of measured, independent and observed [I > 2(I)] reflections |
19532, 7699, 6307 |
|
R
int
|
0.026 |
| (sin /)max (1) |
0.650 |
| |
| Refinement |
|
R[F
2 > 2(F
2)], wR(F
2), S
|
0.040, 0.086, 1.05 |
| No. of reflections |
7699 |
| No. of parameters |
409 |
| No. of restraints |
1 |
| H-atom treatment |
H-atom parameters constrained |
|
max, min (e 3) |
0.22, 0.25 |
| Absolute structure |
Flack x determined using 2415 quotients [(I
+)(I
)]/[(I
+)+(I
)] (Parsons et al., 2013 ▸) |
| Absolute structure parameter |
0.00(3) |
