Table 3. Experimental details.
| Crystal data | |
| Chemical formula | C8H16N4C8H9ClO |
| M r | 324.85 |
| Crystal system, space group | Monoclinic, C2/c |
| Temperature (K) | 173 |
| a, b, c () | 25.6048(18), 7.5295(7), 18.2317(13) |
| () | 111.080(5) |
| V (3) | 3279.7(5) |
| Z | 8 |
| Radiation type | Mo K |
| (mm1) | 0.24 |
| Crystal size (mm) | 0.27 0.26 0.22 |
| Data collection | |
| Diffractometer | Stoe IPDS II two-circle |
| Absorption correction | Multi-scan (X-RED32; Stoe Cie, 2001 ▸) |
| T min, T max | 0.738, 1.000 |
| No. of measured, independent and observed [I > 2(I)] reflections | 14414, 3066, 2512 |
| R int | 0.083 |
| (sin /)max (1) | 0.608 |
| Refinement | |
| R[F 2 > 2(F 2)], wR(F 2), S | 0.040, 0.107, 1.02 |
| No. of reflections | 3066 |
| No. of parameters | 205 |
| H-atom treatment | H atoms treated by a mixture of independent and constrained refinement |
| max, min (e 3) | 0.26, 0.25 |