Table 2. Experimental details.
| Crystal data | |
| Chemical formula | C31H27N4O |
| M r | 471.56 |
| Crystal system, space group | Monoclinic, P21/c |
| Temperature (K) | 123 |
| a, b, c () | 18.5666(8), 20.2009(9), 6.7749(2) |
| () | 92.743(3) |
| V (3) | 2538.10(17) |
| Z | 4 |
| Radiation type | Mo K |
| (mm1) | 0.08 |
| Crystal size (mm) | 0.34 0.12 0.08 |
| Data collection | |
| Diffractometer | Nonius KappaCCD |
| Absorption correction | Multi-scan (Blessing, 1995 ▸) |
| T min, T max | 0.883, 1.078 |
| No. of measured, independent and observed [I > 2(I)] reflections | 35758, 6691, 3221 |
| R int | 0.118 |
| (sin /)max (1) | 0.685 |
| Refinement | |
| R[F 2 > 2(F 2)], wR(F 2), S | 0.049, 0.122, 0.89 |
| No. of reflections | 6691 |
| No. of parameters | 329 |
| H-atom treatment | H-atom parameters constrained |
| max, min (e 3) | 0.19, 0.23 |