| Bruker X8 Proteum diffractometer | 3008 independent reflections |
| Radiation source: Bruker MicroStar microfocus rotating anode | 2601 reflections with I > 2σ(I) |
| Helios multilayer optics monochromator | Rint = 0.041 |
| Detector resolution: 18.4 pixels mm-1 | θmax = 64.4°, θmin = 6.9° |
| φ and ω scans | h = −9→9 |
| Absorption correction: multi-scan (SADABS; Bruker, 2013) | k = −10→10 |
| Tmin = 0.797, Tmax = 0.813 | l = −14→14 |
| 10087 measured reflections |
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