| Agilent Xcalibur Sapphire3 diffractometer | 3449 independent reflections |
| Radiation source: Enhance (Mo) X-ray Source | 2479 reflections with I > 2σ(I) |
| Graphite monochromator | Rint = 0.049 |
| Detector resolution: 16.0560 pixels mm-1 | θmax = 26.0°, θmin = 2.5° |
| ω scans | h = −7→7 |
| Absorption correction: multi-scan (CrysAlis PRO; Agilent, 2013) | k = −15→21 |
| Tmin = 0.782, Tmax = 1.000 | l = −20→20 |
| 9521 measured reflections |
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