| Crystal data |
| Chemical formula |
C17H21ClN2O6
|
|
M
r
|
384.81 |
| Crystal system, space group |
Triclinic, P
|
| Temperature (K) |
293 |
|
a, b, c () |
9.479(5), 10.080(5), 10.320(5) |
| , , () |
108.552(5), 102.886(5), 94.406(5) |
|
V (3) |
899.5(8) |
|
Z
|
2 |
| Radiation type |
Mo K
|
| (mm1) |
0.25 |
| Crystal size (mm) |
0.20 0.15 0.10 |
| |
| Data collection |
| Diffractometer |
Bruker Kappa APEXII CCD |
| Absorption correction |
Multi-scan (SADABS; Bruker, 2008 ▸) |
|
T
min, T
max
|
0.952, 0.976 |
| No. of measured, independent and observed [I > 2(I)] reflections |
12878, 3737, 3025 |
|
R
int
|
0.025 |
| (sin /)max (1) |
0.631 |
| |
| Refinement |
|
R[F
2 > 2(F
2)], wR(F
2), S
|
0.041, 0.121, 1.04 |
| No. of reflections |
3737 |
| No. of parameters |
239 |
| H-atom treatment |
H-atom parameters constrained |
|
max, min (e 3) |
0.25, 0.28 |
